HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 73614Generated: October 29, 2026
(4aS,8aS)-1-benzyl-4-(phenylamino)octahydroquinolin-4a(2H)-ol → HCID 68154084, compound
https://huagongshe.com/reaction/73614
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | (4aS,8aS)-1-benzyl-4-(phenylamino)octahydroquinolin-4a(2H)-ol | HCID 52911548 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68154084 | HCID 68154084 | — |
Reaction Steps
To a mixture of (4aS,8aS)-1-benzyl-4-(phenylamino)octahydroquinolin-4a(2H)-ol (0.280 g, 0.832 mmol) in MeOH (5 mL) was added NH4COOH (0.840 g, 13.3 mmol) and 10% Pd/C (0.280 g). The resulting mixture was heated at 60° C. for several hours. The reaction was cooled to rt, filtered through a syringe filter, washed with EtOH, and concentrated to give the title compound. LRMS M+H calc'd: 247.34. found 247.34
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08829196B2 |
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| Source dataset | uspto-grants-2014_09 |
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| ORD ID | ord-4f198c0a3a474dfe812baf3eda919d30 |
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| Source note | uspto-grants-2014_09 |
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