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HRID736309

反应详情

EQUATION

反应方程式

HRID 736309 的结构方程式

REACTANTS

反应物

2
结构：CN(C)C=CC(=O)c1cccnc1
HCID567033

3-Dimethylamino-1-(3-pyridyl)-2-propen-1-one

C10H12N2O

结构：N=C(N)Nc1cccc([N+](=O)[O-])c1.O=[N+]([O-])O
HCID178512513

未命名化合物

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1cccc(Nc2nccc(-c3cccnc3)n2)c1
HCID9860872

未命名化合物

收率 69.7%

PROCEDURE

实验过程

3-Nitrophenyl-guanidine nitrate (28 g, 0.12 mol) and 3-dimethylamino-1-(3-pyridyl)-2-propen-1-one (16.9 g, 0.09 mol) were reacted according to the same procedure as Step 1.3 of Preparation 1 to give N-(3-nitrophenyl)-4-(3-pyridyl)-2-pyrimidine-amine (18.4 g).

WORKUP

后处理

  1. customaccording to the same procedure as Step 1.3 of Preparation 1