HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23435828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-[(2-Oxooxolan-3-yl)oxy]-1H-isoindole-1,3(2H)-dione | HCID 13577114 | — |
| Product | HCID 23435828 | HCID 23435828 | — |
Reaction Steps
α-Phthalimidooxy-γ-butyrolactone (1.0 g, 4 mmol) was added to hydrochloric acid (1 M, 10 mL) at reflux. After 5 min. at reflux for 5 min and the reaction was cooled down on an ice bath and filtered. The filtrate was evaporated to dryness. Toluene was added and residual water removed azeotropic distillation. 0.75 g of the desired material was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595336B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-4adeacfeef7b4b7cac76b904a38d3139 |
| Source note | uspto-grants-2009_09 |