HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57849365, compound → HCID 57849355, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57849365 | HCID 57849365 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57849355 | HCID 57849355 | 94% |
Reaction Steps
Acetic acid 1-{4-[1-(4-benzyloxy-3-methyl-phenyl)-1-ethyl-propyl]-2-methyl-phenoxymethyl}-1-ethyl-propyl ester (0.14 g g, 0.27 mmol), EtOH (20 ml), and 10% Pd/C (25 mg) is hydrogenated at atmospheric pressure for 18 h. The reaction is filtered through diatomaceous earth with EtOAc wash. The filtrate is concentrated to give the title compound (0.11 g, 0.25 mmol, 94%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595345B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-a037dce87807423bb62d86d1ded96206 |
| Source note | uspto-grants-2009_09 |