HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenebutanamine → (4-Isocyanatobutyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenebutanamine | HCID 83242 | — |
| Reactant | Isocyanate | HCID 105034 | — |
| Product | (4-Isocyanatobutyl)benzene | HCID 15932353 | 84% |
Reaction Steps
Following the synthetic procedure of 4b′ as described in Example 17, isocyanate 4c′ (84% yield) was synthesized from 4-(phenyl)butylamine as an oil. 1H-NMR (CDCl3) δ1.61-1.78 (m, 4H), 2.66 (t, J=7.5 Hz, 2H), 3.32 (t, J=6.5 Hz, 2H), 7.17-7.23 (m, 3H), 7.26-7.32 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595403B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-506b2c1120fe449891f5b23ec1c9f03e |
| Source note | uspto-grants-2009_09 |