HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 68817317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 68818823 | HCID 68818823 | — |
| Product | HCID 68817317 | HCID 68817317 | 39.2% |
Reaction Steps
According to the procedure of Example 17, Step 3, the reaction of 320.4 mg of tert-butyl cis-4-[({4-[(2-methylquinolin-4-yl)methoxy]phenyl}sulfonyl)amino]pyrrolidine-3-carboxylate hydrochloride with 57 mg of acetyl chloride provided 127 mg (39% yield) of tert-butyl cis-1-acetyl-4-[({4-[(2-methylquinolin-4-yl)methoxy]phenyl}sulfonyl)amino]pyrrolidine-3-carboxylate. MS: 540.1(M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595327B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-78b7e8a09eb041f68d2ea39a17d8393b |
| Source note | uspto-grants-2009_09 |