HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → HCID 86607881, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | HCID 68817491 | HCID 68817491 | — |
| Product | HCID 86607881 | HCID 86607881 | 11% |
Reaction Steps
According to the procedure of Example 24, Step 3, 4-[4-(2-methyl-quinolin-4-ylmethoxy)-benzenesulfonylamino]-tetrahydro-furan-3-carboxylic acid (0.6 g, 1.35 mmol) and hydroxylamine afforded (3S,4R)-4-[4-(2-methyl-quinolin-4-ylmethoxy)-benzenesulfonylamino]-tetrahydro-furan-3-carboxylic acid hydroxyamide as an amorphous white solid (0.07 g, 11%) after HPLC purification, eluting with acetonitrile:water. MS: 458 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595327B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-ac54edac97b346dc831c25cce8c6cbb3 |
| Source note | uspto-grants-2009_09 |