HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetaldehyde → 2-[2-(2-Phenylethenyl)hydrazinyl]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetaldehyde | HCID 998 | — |
| Reactant | 2-Hydrazinopyridine | HCID 78645 | — |
| Product | 2-[2-(2-Phenylethenyl)hydrazinyl]pyridine | HCID 68874495 | 100% |
Reaction Steps
React Pyridin-2-yl-hydrazine and Phenyl-acetaldehyde under literature conditions (Azaindoles. I. Preparation of 7-azaindoles by thermal indolization of 2-pyridylhydrazones. Canadian Journal of Chemistry (1966), 44(21), 2455-9) to give N-Pyridin-2-yl-N′-styryl-hydrazine (10 g, 100% yield crude material) Mass Spectrum (m/e): 211.96 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595339B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-a775497ccd2d462c92ab1aa5a0d9059e |
| Source note | uspto-grants-2009_09 |