HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 57849488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Bromobenzyl bromide | HCID 68527 | — |
| Reactant | (2S)-2-Phenylmorpholine | HCID 937783 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 57849488 | HCID 57849488 | 68% |
Reaction Steps
1.417 g of 4-Bromobenzyl bromide and 0.617 g of (S)-2-Phenyl-morpholine in 11 mL of acetonitrile were stirred at room temperature and 1.567 g of potassium carbonate was added. The reaction was stirred at room temperature overnight. The solution was filtered through Celite and concentrated in vacuo to afford a brown solid. Purification by flash chromatography afforded 0.851 g of product. 68% yield ES MS m/z 331.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595397B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-25ee7b7d635e4fbd842faa1bbeba7652 |
| Source note | uspto-grants-2009_09 |