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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 737073Generated: October 30, 2026

Potassium Carbonate → HCID 57849488, compound

https://huagongshe.com/reaction/737073

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant4-Bromobenzyl bromideHCID 68527—
Reactant(2S)-2-PhenylmorpholineHCID 937783—
SolventAcetonitrileHCID 6342—
ProductHCID 57849488HCID 5784948868%

Reaction Steps

1.417 g of 4-Bromobenzyl bromide and 0.617 g of (S)-2-Phenyl-morpholine in 11 mL of acetonitrile were stirred at room temperature and 1.567 g of potassium carbonate was added. The reaction was stirred at room temperature overnight. The solution was filtered through Celite and concentrated in vacuo to afford a brown solid. Purification by flash chromatography afforded 0.851 g of product. 68% yield ES MS m/z 331.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07595397B2
Source datasetuspto-grants-2009_09
ORD IDord-25ee7b7d635e4fbd842faa1bbeba7652
Source noteuspto-grants-2009_09