Potassium Carbonate → HCID 57849518, compound

Participants

Reaction Steps

5.632 g of 4-Bromobenzyl bromide and 2.694 g of 2-Phenylthiomorpholine (Array) in 50 mL of acetonitrile were stirred at room temperature and 6.229 g of potassium carbonate was added. The reaction was stirred at room temperature overnight. The solution was filtered through Celite and concentrated in vacuo to afford a brown solid. Purification was done by flash chromatography to afford product. Wt: 0.859 g, 53% yield. ES MS m/z 348/350

Provenance & Evidence