Ethanolamine → HCID 55298746, compound

HRID 737106Notes

Reaction equation

HRID 737106 reaction equation
O1CC1[CH2:3][C:4]12[O:10][CH:5]1[CH:6]=CC=[CH:9]2.[CH2:12]([CH2:14][NH2:15])[OH:13]>O>[OH:13][CH2:12][CH2:14][NH:15][CH2:6][CH:5]([OH:10])[CH:4]([CH3:3])[CH3:9]

Participants

4

Reactant 2

HCID 700EthanolamineHCID 86614311HCID 86614311, compound

Product 1

HCID 55298746HCID 55298746, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The above compound could be made in the same manner as Example 1 using the appropriate epoxide: 1 eq. of (2,3-Epoxypropyl)benzene oxide and 4 eq. ethanol amine The above compound could be made in the following manner: stirred at room temperature overnight. The solution could be poured into water and the water is extracted with dichloromethane. The combined dichloromethane layers could be washed with brine and concentrated.

Workup

  1. extractionthe water is extracted with dichloromethane
  2. washThe combined dichloromethane layers could be washed with brine
  3. concentrationconcentrated

Sources & evidence

ORD record
ord-09b69d85226c4bcbabcebd2394918ac3
Source dataset
uspto-grants-2009_09
Patent number
US07595397B2

Reaction notes

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