HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 57849627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Bromobenzyl bromide | HCID 68527 | — |
| Reactant | 2-(Propan-2-yl)morpholine | HCID 19877688 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 57849627 | HCID 57849627 | — |
Reaction Steps
The above compound could be made in the following manner: 1.5 eq. of 4-Bromobenzyl bromide and 1 eq. of 2-Isopropyl-morpholine in acetonitrile could be stirred at room temperature and 3 eq. of potassium carbonate could be added. The reaction could be stirred at room temperature overnight. The solution could be filtered through Celite and concentrated in vacuo to afford a brown solid. Purification could be done by flash chromatography to afford product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07595397B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-f76af3ff5147415eb43327fcda4bf1bd |
| Source note | uspto-grants-2009_09 |