反应详情

Thiourea (0.47 g, 6.2 mmol) and NaOAc (1.5 g, 6.2 mmol) were combined in 35 mL of ethanol. To this suspension was added 4-(2-bromo-acetyl)-benzoic acid (1.5 g, 6.2 mmol). The reaction mixture was stirred at room temperature overnight. It was evaporated to dryness and used in the next step without any further purification. MS: 221.0 (M+H+)

1. customIt was evaporated to dryness
2. customused in the next step without any further purification