HRID737194

反应详情

EQUATION

反应方程式

HRID 737194 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

4-(2-Bromo-acetyl)-N-cyclopentyl-benzenesulfonamide (150 mg, 0.43 mmol) was combined with thiourea (33 mg, 0.43 mmol) in 7 ml of dry EtOH. To this solution was added NaOAc (53 mg, 0.65 mmol). Reaction mixture was stirred at room temperature for 4 hours. Reaction mixture was evaporated to dryness and used in the next step without further purification.

WORKUP

后处理

  1. customReaction mixture
  2. customReaction mixture
  3. customwas evaporated to dryness
  4. customused in the next step without further purification