HRID73772

反应详情

EQUATION

反应方程式

HRID 73772 的结构方程式

PROCEDURE

实验过程

The title compound was prepared in an analogous fashion to that described in Stage 11.2 using 5-bromo-6-chloro-nicotinic acid and 4-aminophenylsulfur pentafluoride to afford an orange solid. HPLC (Condition 4), tR=6.43 min, UPLC-MS (Condition 3), tR=1.27 min, m/z=435.3/437.2 [M+H]+.

WORKUP

后处理

  1. customto afford an orange solid