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HRID73805

反应详情

EQUATION

反应方程式

HRID 73805 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1cnc(Cl)c(Br)c1
HCID285433

5-bromo-6-chloronicotinic acid

C6H3BrClNO2

结构：Nc1ccc(SC(F)(F)F)nc1
HCID43625022

未命名化合物

PRODUCTS

生成物

1
结构：O=C(Nc1ccc(SC(F)(F)F)nc1)c1cnc(Cl)c(Br)c1
HCID86702634

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in an analogous fashion to that described in Stage 9.3 using 5-bromo-6-chloronicotinic acid and 6-(trifluoromethylthio)pyridin-3-amine to afford an off-white powder. HPLC (Condition 4) tR=6.43 min, UPLC-MS (Condition 3) tR=1.15 min, m/z=411.9 [M−H]−.

WORKUP

后处理

  1. customto afford an off-white powder