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HRID73934

反应详情

EQUATION

反应方程式

HRID 73934 的结构方程式

REACTANTS

反应物

2
结构：CCC(C)Br
HCID6554

2-Bromobutane

C4H9Br

结构：O=[N+]([O-])c1ccc2cc[nH]c2c1
HCID78502

6-Nitro-1H-indole

C8H6N2O2

PRODUCTS

生成物

1
结构：CCC(C)c1c[nH]c2cc(N)ccc12
HCID57470200

3-(1-Methylpropyl)-1H-indol-6-amine

C12H16N2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

3-sec-Butyl-1H-indol-6-ylamine (B-14) was synthesized following the general scheme above starting from 6-nitroindole and 2-bromobutane. Overall yield (20%). HPLC ret. time 2.32 min, 10-99% CH3CN, 5 min run; ESI-MS 189.5 m/z (MH+).

WORKUP

后处理

  1. customOverall yield (20%)