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HRID74025

反应详情

EQUATION

反应方程式

HRID 74025 的结构方程式

REACTANTS

反应物

1
结构：O=[N+]([O-])c1ccc(OC(F)(F)F)c([N+](=O)[O-])c1
HCID2737131

2,4-Dinitro-1-(trifluoromethoxy)benzene

C7H3F3N2O5

PRODUCTS

生成物

1
结构：Nc1ccc(OC(F)(F)F)c(N)c1
HCID24902286

4-(Trifluoromethoxy)benzene-1,3-diamine

C7H7F3N2O

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

4-Trifluoromethoxy-benzene-1,3-diamine (D-4) was synthesized following the general scheme above starting from 2,4-dinitro-1-trifluoromethoxy-benzene. Yield (89%). HPLC ret. time 0.91 min, 10-99% CH3CN, 5 min run; ESI-MS 193.3 m/z (MH+).

WORKUP

后处理

  1. customYield (89%)