HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Indole-3-carbonyl chloride → HCID 131719521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Indole-3-carbonyl chloride | HCID 12380278 | — |
| Reactant | HCID 67836758 | HCID 67836758 | — |
| Product | HCID 131719521 | HCID 131719521 | — |
Reaction Steps
eq-2-(2-Hydroxyethyl)quinolizidine (D5) was reacted with indole-3-carboxylic acid chloride using the method of Example 1. The product was chromatographed on silica gel eluting with ethyl acetate/methanol (95:5). The resulting beige solid was recrystallised from ethyl acetate/petrol (60-80) to afford the title compound (E10) as a white solid mp 170°-172° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05552398 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-4e97cdcc392d4a489d1f38aa1389f237 |
| Source note | uspto-grants-1996_09 |