HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 558152, compound → HCID 131719522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 558152 | HCID 558152 | — |
| Reactant | 1H-Indole-3-carbonyl chloride | HCID 12380278 | — |
| Product | HCID 131719522 | HCID 131719522 | — |
Reaction Steps
eq-1-Hydroxyquinolizidine (H. S. Aaron et al, J. Org. Chem. 1964, 29, 2248) was reacted with indole-3-carboxylic acid chloride using the method of Example 1. The product was chromatographed on silica gel eluting with ether to afford the title compound (E11a) as a white solid, mp 230°-232° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05552398 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-1832583900084f838cfa49da50a1aa16 |
| Source note | uspto-grants-1996_09 |