1-(2-Chloroethyl)piperidine → HCID 19353994, compound

HRID 741746Notes

Reaction equation

HRID 741746 reaction equation
[Br:1][C:2]1[CH:30]=[CH:29][CH:28]=[CH:27][C:3]=1[CH2:4][N:5]1[C:9]2[CH:10]=[C:11]([OH:14])[CH:12]=[CH:13][C:8]=2[N:7]=[C:6]1[C:15]1[CH:20]=[C:19]([O:21][CH3:22])[C:18]([O:23][CH3:24])=[C:17]([O:25][CH3:26])[CH:16]=1.[N:31]1([CH2:37][CH2:38]Cl)[CH2:36][CH2:35][CH2:34][CH2:33][CH2:32]1>>[Br:1][C:2]1[CH:30]=[CH:29][CH:28]=[CH:27][C:3]=1[CH2:4][N:5]1[C:9]2[CH:10]=[C:11]([O:14][CH2:38][CH2:37][N:31]3[CH2:36][CH2:35][CH2:34][CH2:33][CH2:32]3)[CH:12]=[CH:13][C:8]=2[N:7]=[C:6]1[C:15]1[CH:16]=[C:17]([O:25][CH3:26])[C:18]([O:23][CH3:24])=[C:19]([O:21][CH3:22])[CH:20]=1

Participants

3

Reactant 2

HCID 748271-(2-Chloroethyl)piperidineHCID 19354036HCID 19354036, compound

Product 1

HCID 19353994HCID 19353994, compound

Procedure

The title compound was prepared by reacting the compound of Example 114 with 2-(piperidin-1-yl)ethyl chloride essentially as previously described. mp 145° C., NMR, MS 579, 581, IR.

Sources & evidence

ORD record
ord-60347eebea6644cebe31bd8628d12dde
Source dataset
uspto-grants-1996_09
Patent number
US05552426

Reaction notes

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