3-Chloro-N,N-dimethyl-1-propanamine → HCID 19354022, compound

HRID 741749Notes

Reaction equation

HRID 741749 reaction equation
[Br:1][C:2]1[CH:30]=[CH:29][CH:28]=[CH:27][C:3]=1[CH2:4][N:5]1[C:9]2[CH:10]=[C:11]([OH:14])[CH:12]=[CH:13][C:8]=2[N:7]=[C:6]1[C:15]1[CH:20]=[C:19]([O:21][CH3:22])[C:18]([O:23][CH3:24])=[C:17]([O:25][CH3:26])[CH:16]=1.[CH3:31][N:32]([CH2:34][CH2:35][CH2:36]Cl)[CH3:33]>>[Br:1][C:2]1[CH:30]=[CH:29][CH:28]=[CH:27][C:3]=1[CH2:4][N:5]1[C:9]2[CH:10]=[C:11]([O:14][CH2:36][CH2:35][CH2:34][N:32]([CH3:33])[CH3:31])[CH:12]=[CH:13][C:8]=2[N:7]=[C:6]1[C:15]1[CH:16]=[C:17]([O:25][CH3:26])[C:18]([O:23][CH3:24])=[C:19]([O:21][CH3:22])[CH:20]=1

Participants

3

Reactant 2

HCID 669603-Chloro-N,N-dimethyl-1-propanamineHCID 19354036HCID 19354036, compound

Product 1

HCID 19354022HCID 19354022, compound

Procedure

The title compound was prepared by reacting the compound of Example 114 with 3-(N,N-dimethylamino)propyl chloride essentially as previously described. mp 141° C., NMR, IR, MS 553, 555.

Sources & evidence

ORD record
ord-8b174e8e4adf489b87a1bbfdf048f95e
Source dataset
uspto-grants-1996_09
Patent number
US05552426

Reaction notes

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