HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-N,N-dimethylethylamine → 1-(2-bromobenzyl)-2-(3-methylphenyl)-6-[2 (N,N-dimethylamino)ethoxy]benzimidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-N,N-dimethylethylamine | HCID 7901 | — |
| Reactant | 1-(2-Bromobenzyl)-2-(3-methylphenyl)-6hydroxybenzimidazole | HCID 19353935 | — |
| Product | 1-(2-bromobenzyl)-2-(3-methylphenyl)-6-[2 (N,N-dimethylamino)ethoxy]benzimidazole | HCID 19353946 | — |
Reaction Steps
The title compound was prepared essentially as described in Example 117 except that the compound of Example 126 was reacted with 2-(N,N-dimethylamino)ethyl chloride. mp 71° C., NMR, IR, MS 464, 466.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05552426 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-268377b5942843afb9b178b9b2103714 |
| Source note | uspto-grants-1996_09 |