Triethylene glycol monomethyl ether → HCID 19427130, compound

Participants

Reaction Steps

The procedure of Example 1 was repeated with 151.8 g (0.50 mole) of dodecyltrichlorosilane and 200 g. of heptane. Under nitrogen 254.2 g (1.55 mole) of 2-(2-(2-methoxyethoxy)ethoxy)ethanol was added over 3 hours at 80° C. followed by heating of the reaction for an additional 48 hours. Vacuum stripping of all volatiles left 350 g of the clear, pale yellow liquid product.

Provenance & Evidence