Trichlorooctadecylsilane → 12-[2-[2-(2-Methoxyethoxy)ethoxy]ethoxy]-12-octadecyl-2,5,8,11,13,16,19,22-octaoxa-12-silatricosane

Beteiligte Stoffe

Reaktionsschritte

The procedure of Example 1 was repeated with 387.5 g (1.0 mole) of octadecyltrichlorosilane and 800 mL of heptane. Under nitrogen 508.4 g (3.10 mole) of 2-(2-(2-methoxyethoxy)ethoxy)ethanol was added at 80° C. over 4 hours. After heating the reaction for an additional 48 hours and removal of all volatile components under vacuum, 780 g of the pale yellow liquid product were obtained.

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