HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → 2-Bromo-6-(tert-butyldiphenylsiloxy)methylpyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | 3-Bromophenol | HCID 11563 | — |
| Reactant | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| Reactant | 6-Bromopyridine-2-carboxylic acid | HCID 593919 | — |
| Product | 2-Bromo-6-(tert-butyldiphenylsiloxy)methylpyridine | HCID 23370237 | — |
Reaction Steps
Following the procedure described for Phenol 7, Step 1 but substituting tert-butyldiphenylsilyl chloride for tert-butyldimethylsilyl chloride and 6-bromopyridin-2-methanol from Step 1 for 3-bromophenol, the title compound was obtained as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05552437 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-949cbe8468a445e995697b78f7a65a66 |
| Source note | uspto-grants-1996_09 |