HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → 6-(3-Hydroxypent-3-yl)pyridin-2-methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | 1-Bromo-3-(3,4-dimethoxybenzyloxy)-5-fluorobenzene | HCID 19426985 | — |
| Reactant | 2-Bromo-6-(tert-butyldiphenylsiloxy)methylpyridine | HCID 23370237 | — |
| Product | 6-(3-Hydroxypent-3-yl)pyridin-2-methanol | HCID 19426993 | — |
Reaction Steps
Following the procedure described for Phenol 2, Step 2 and for Phenol 7, Step 3, but substituting 6-bromo(O-tert-butyldiphenylsilyl)pyridin-2-methanol form Step 4 for 1-bromo-3-(3,4-dimethoxybenzyloxy)-5-fluorobenzene, the title compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05552437 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-5323fae251334457994cf16671f58341 |
| Source note | uspto-grants-1996_09 |