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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 742271생성일: 2026년 10월 25일

Triethylamine → 3-(2-Ethyl-6-methylphenyl)-1-isopropyl-2-thioxo-imidazolidin-4-one

https://huagongshe.com/reaction/742271

반응식

참여 물질

역할이름HCID투입량
반응물TriethylamineHCID 8471—
반응물2-Ethyl-6-methylphenyl isothiocyanateHCID 144188—
반응물NoName_76HCID 414244—
용매ChloroformHCID 6212—
생성물3-(2-Ethyl-6-methylphenyl)-1-isopropyl-2-thioxo-imidazolidin-4-oneHCID 8570153147.1%

반응 단계

The title compound was prepared by the procedure described in Example 45 using 17.7 g of 2-ethyl-6-methylphenyl-isothiocyanate, 21.2 g of N-isopropyl glycine, 21.0 g of triethyl amine, and 300 mL of chloroform. Crystallization from ethanol afforded the title compound (13.0 g) as a light yellow solid, m.p. 132°-134° C. Anal. Calcd. for. C15H2O N2O S: C, 65.18; H, 7.29; N, 10.14. Found: C, 65.06; H, 7.37; N, 10.20. Mass spectrum (El, M.+) m/z 276.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05554607
출처 데이터셋uspto-grants-1996_09
ORD IDord-d62e6f8eb9d84c96b8eb7285ba8bb833
출처 메모uspto-grants-1996_09