HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → HCID 178508989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178508962 | HCID 178508962 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178508989 | HCID 178508989 | 78% |
Reaction Steps
Following the procedure of Example 16 but substituting 21.4 g. (0.113 M) of 2-amino-6-phenyl-4-pyrimidinol, 200 ml. water, 500 ml. chloroform, 5.6 g. sodium hydroxide and 28.8 g. I2, a yield of 29.0 g. (78%) of 2-amino-5-iodo-6-phenyl-4-pyrimidinol is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05554617 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-47966da42302449184fa33cebf8a2382 |
| Source note | uspto-grants-1996_09 |