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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 742342Generated: November 1, 2026

Benzeneseleninic acid → HCID 54465294, compound

https://huagongshe.com/reaction/742342

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzeneseleninic acidHCID 23427—
ReactantHCID 19425972HCID 19425972—
SolventTolueneHCID 1140—
ProductHCID 54465294HCID 54465294—

Reaction Conditions

Temperature70 °C

Reaction Steps

49a (0.68 g, 2.26 mmol) in toluene (5 ml) was added benzeneseleninic acid (0.64 g, 3.39 mmol). The mixture was heated to 70° C. for 5 hours. After cooling the product was filtered off and washed with warm toluene and CH2Cl2 successively. Yield 0.58 g (86%). Mp 200°-202° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05554630
Source datasetuspto-grants-1996_09
ORD IDord-486b7310a2b943e5887728119ad1766e
Source noteuspto-grants-1996_09