HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid monohydrate → HCID 19047547, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | HCID 19047540 | HCID 19047540 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19047547 | HCID 19047547 | 61.7% |
Reaction Steps
To a mixture of 5 g (0.024 mol) of 1-(3-furyl)-indan-1-ol in 500 mL of toluene was added 50 mg of p-toluenesulfonic acid monohydrate and the solvent was distilled in vacuo (40 mm) until a residue was obtained. The residue was chromatographed (silica, 1:1 hexane/methylene chloride) to afford 2.7 g (61.3%) of 1-(3-furyl)-indene as a clear oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05554620 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-7ea84f964bd84ac789b22206f731ff75 |
| Source note | uspto-grants-1996_09 |