Thionyl Chloride → HCID 19047521, compound

HRID 742492Notes

Reaction equation

[CH2:1]([O:3][C:4]([C:6]([CH3:12])([CH3:11])[CH2:7][C:8](O)=[O:9])=[O:5])[CH3:2].S(Cl)([Cl:15])=O>>[CH2:1]([O:3][C:4]([C:6]([CH3:12])([CH3:11])[CH2:7][C:8]([Cl:15])=[O:9])=[O:5])[CH3:2]

Participants

Reactant 2

HCID 24386Thionyl Chloride

HCID 1429488732980-28-2

Product 1

HCID 19047521HCID 19047521, compound

Procedure

A mixture of 3-ethoxycarbonyl-3,3-dimethylpropionic acid (1 g) and 3 ml of thionyl chloride was stirred at room temperature for 20 hours. The excess thionyl chloride was removed in vacuo to afford 1.1 g of 3-ethoxycarbonyl-3,3-dimethylpropionyl chloride.

Workup

customThe excess thionyl chloride was removed in vacuo

Sources & evidence

ORD record: ord-6be85a7089ba4a5c95b68c1e86a42a63
Source dataset: uspto-grants-1996_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05554620

Reaction notes

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