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HRID742508

反应详情

EQUATION

反应方程式

HRID 742508 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：CCCCCCCCOC(=O)C(C)C(C)(C)C(=O)O
HCID19047496

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCOC(=O)C(C)C(C)(C)C(=O)Cl
HCID53899365

未命名化合物

PROCEDURE

实验过程

3-(1-Octyloxycarbonyl)-2,2-dimethylbutyric acid (0.4 g) was treated with thionyl chloride (20 ml) and the excess thionyl chloride was removed in vacuo to afford 0.33 g of 3-(1-octyloxycarbonyl)-2,2-dimethylbutyric acid chloride.

WORKUP

后处理

  1. customthe excess thionyl chloride was removed in vacuo