HRID742611

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID265934

dimethyl hydrazine-1,2-dicarboxylate

C4H8N2O4

HCID11322811

1-cyclohexyloxy-2,2,6,6-tetramethyl-piperidin-4-ol

C15H29NO2

PRODUCTS

生成物

结构：CC1(C)CC(OC(=O)NNC(=O)OC2CC(C)(C)N(OC3CCCCC3)C(C)(C)C2)CC(C)(C)N1OC1CCCCC1

HCID54341087

未命名化合物

收率 54.5%

AUXILIARIES

试剂、催化剂与溶剂

结构：CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-].[Ti+4]

催化剂HCID21801

Titanium(IV) n-butoxide

C16H36O4Ti

PROCEDURE

实验过程

The procedure of Example 1 is repeated using 24.1 g of 1-cyclohexyloxy-2,2,6,6-tetramethylpiperidin-4-ol, 6.67 g of dimethyl hydrazine-1,2-dicarboxylate and 1.5 g of tetrabutyl titanate to afford 14.6 g of the title compound as a white solid; mp 150°-152° C.