HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octahydro-2H-azonin-2-one → Perhydroazonine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octahydro-2H-azonin-2-one | HCID 13632 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Perhydroazonine | HCID 79742 | 90% |
Reaction Steps
Caprylolactam (Fluka, N.Y., #21631) (25 g, 117 mmoles) is combined with lithium aluminum hydride (10.5 g) in ether and reduced with stirring for 5 hr. The reaction mixture is filtered and evaporated with ether. The product is octahydroazonin (90% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556840 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-7f74f44fe6f048a1a856793572bfd947 |
| Source note | uspto-grants-1996_09 |