N,N-Diethylethylenediamine → HCID 19423536, compound

HRID 743072Notes

Reaction equation

HRID 743072 reaction equation
[N+:1]([C:4]1[CH:5]=[CH:6][C:7]([NH:18][C:19](=[O:24])C(Cl)(Cl)Cl)=[C:8]([CH:17]=1)[C:9]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=O)([O-:3])=[O:2].[CH2:25]([N:27]([CH2:31][CH3:32])[CH2:28][CH2:29][NH2:30])[CH3:26]>>[CH2:25]([N:27]([CH2:31][CH3:32])[CH2:28][CH2:29][N:30]1[CH:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[C:8]2[C:7](=[CH:6][CH:5]=[C:4]([N+:1]([O-:3])=[O:2])[CH:17]=2)[NH:18][C:19]1=[O:24])[CH3:26]

Participants

3

Reactant 2

HCID 60993N,N-DiethylethylenediamineHCID 4702294HCID 4702294, compound

Product 1

HCID 19423536HCID 19423536, compound

Procedure

In similar way as in Preparation Example 1, the title compound was synthesized from 5-nitro-2-trichloroacetylaminobenzophenone and 2-(diethylamino)ethylamine.

Workup

  1. customIn similar way as in Preparation Example 1

Sources & evidence

ORD record
ord-94429cf443ef48f8ac25c4f85f3acf48
Source dataset
uspto-grants-1996_09
Patent number
US05556860

Reaction notes

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