Epibromohydrin → HCID 19424026, compound

Participants

Reaction Steps

Following a procedure similar to that described in Example 1(a), 2.87 g of 2-[4-(3-methoxymethoxyphenyl)butyl]phenol (prepared as described in Preparation 5), 1.18 g of potassium t-butoxide and 1.67 g of epibromohydrin were reacted in 30 ml of dimethylacetamide. The crude product, extracted as described in Example 1(a), was purified as described in Example 1(a), to give 2.05 g (yield 60%) of the title compound as a colorless oil.

Provenance & Evidence