HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 10786777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 10519198 | HCID 10519198 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 10786777 | HCID 10786777 | 93% |
Reaction Steps
Following a procedure similar to that described in Example 1(b), 208 mg of 2-{2-[4-(4-methoxyphenyl)butyl]phenoxymethyl}oxirane [prepared as described in step (a) above] dissolved in 5 ml of tetrahydrofuran were treated with 1 ml of 50% by volume aqueous dimethylamine. The crude product was purified as described in Example 1(b), to give 223 mg (yield 93%) of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556864 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-8a271cc56a134e4290dde2486a93516a |
| Source note | uspto-grants-1996_09 |