HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epibromohydrin → HCID 19424029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epibromohydrin | HCID 18430 | — |
| Reactant | HCID 19423889 | HCID 19423889 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 19424029 | HCID 19424029 | 80% |
Reaction Steps
Following a procedure similar to that described in Example 1(a), 329 mg of 2-[4-(1-naphthyl)butyl]phenol (prepared as described in Preparation 16), 134 mg of potassium t-butoxide and 334 mg of epibromohydrin were reacted in 15 ml of dimethylacetamide. The crude product, extracted as described in Example 1(a), was purified as described in Example 1(a), to give 316 mg (yield 80%) of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556864 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-cf8d990ef6244c2a8b5e95f90b06fc6c |
| Source note | uspto-grants-1996_09 |