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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 743231Generated: November 3, 2026

Epibromohydrin → HCID 19424029, compound

https://huagongshe.com/reaction/743231

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEpibromohydrinHCID 18430—
ReactantHCID 19423889HCID 19423889—
ReactantPotassium tert-butoxideHCID 23665647—
SolventDimethylacetamideHCID 31374—
ProductHCID 19424029HCID 1942402980%

Reaction Steps

Following a procedure similar to that described in Example 1(a), 329 mg of 2-[4-(1-naphthyl)butyl]phenol (prepared as described in Preparation 16), 134 mg of potassium t-butoxide and 334 mg of epibromohydrin were reacted in 15 ml of dimethylacetamide. The crude product, extracted as described in Example 1(a), was purified as described in Example 1(a), to give 316 mg (yield 80%) of the title compound as a colorless oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05556864
Source datasetuspto-grants-1996_09
ORD IDord-cf8d990ef6244c2a8b5e95f90b06fc6c
Source noteuspto-grants-1996_09