HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67317226, compound → HCID 25255697, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67317226 | HCID 67317226 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 25255697 | HCID 25255697 | — |
Reaction Steps
Deprotection of 2-(2-(3-(2-propylpentyloxy)phenoxy)ethyl)isoindoline-1,3-dione following the method used in Example 18 gave Example 25 as a colorless oil. Yield (0.11 g, 82%): 1H NMR (400 MHz, DMSO) δ 7.11 (t, J=8.0 Hz, 1H), 6.42-6.48 (m, 3H), 3.85 (t, J=5.6 Hz, 2H), 3.78 (d, J=6.0 Hz, 2H), 2.81 (t, J=6.0 Hz, 2H), 1.65-1.75 (m, 1H), 1.48 (brs, 2H), 1.20-1.40 (m, 8H), 0.85 (t, J=7.2 Hz, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08829244B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-6181f5d67f1b4953976257bd06575889 |
| Source note | uspto-grants-2014_09 |