HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzhydryl-3-(cyclopropylamino)azetidine dihydrochloride → 3-(Cyclopropylamino)azetidine dihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzhydryl-3-(cyclopropylamino)azetidine dihydrochloride | HCID 19423671 | — |
| Reactant | N-ethylazetidin-3-amine dihydrochloride | HCID 22121198 | — |
| Product | 3-(Cyclopropylamino)azetidine dihydrochloride | HCID 19423659 | — |
Reaction Steps
3-(Cyclopropylamino)azetidine dihydrochloride was prepared under the conditions described in Example 9 for 3-(ethylamino)azetidine dihydrochloride, but starting with 5.4 g of 1-benzhydryl-3-(cyclopropylamino)azetidine dihydrochloride. 2.25 g of 3-(cyclopropylamino)azetidine dihydrochloride are obtained in the form of a colorless solid, melting point 140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556861 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-0baaa8c154c04ed3957758a64f01c626 |
| Source note | uspto-grants-1996_09 |