HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22865527, compound → HCID 22865526, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22865527 | HCID 22865527 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 22865526 | HCID 22865526 | — |
Reaction Steps
4-N-(2-Acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranosyl)-L-asparagine tert.-butyl ester (Cornpound 11) The N-Z-protected compound 7 (2.2 g) was hydrogenated in the presence of Pd/C and worked up as described above. Yield: 1.63 g. TLC analysis: Rf=0.47 (chloroform/methanol 6:1 )
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05556941 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-749640439305454eaa19a7203a32da96 |
| Source note | uspto-grants-1996_09 |