HRID743925

反应详情

EQUATION

反应方程式

HRID 743925 的结构方程式

PROCEDURE

实验过程

Using p-tert-butoxystyrene (81.1 g, 0.46 mole) and styrene (4.6 g, 0.04 mole), the polymerization and the treatment were carried out in the same manner as described in Synthesis Example 1, (1), to give 77.1 g of poly(p-tert-butoxystyrene/styrene) as white powders having Mw 20000 (GPC with polystyrene calibration). The polymer was found to have p-tertbutoxystyrene unit and styrene unit in a molar ratio of ca. 92:8 based on 1HNMR.

WORKUP

后处理

  1. customthe polymerization
  2. customas described in Synthesis Example 1, (1),