HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorostyrene → HCID 86749845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorostyrene | HCID 14085 | — |
| Reactant | 1-(Tert-butoxy)-4-ethenylbenzene | HCID 577531 | — |
| Product | HCID 86749845 | HCID 86749845 | — |
Reaction Steps
Using p-tert-butoxystyrene (83.7 g, 0.475 mole) and p-chlorostyrene (3.5 g, 0.025 mole), the polymerization and the treatment were carried out in the same manner as described in Synthesis Example 1, (1), to give 75.9 g of poly(p-tert-butoxystyrene/p-chlorostyrene) as white powder having Mw 22000 (GPC with polystyrene calibration). The polymer was found to have p-tert-butoxystyrene unit and p-chlorostyrene unit in a molar ratio of ca. 95:5 based on 1HNMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05558976 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-167f2ffa4b864eb78eb65bbfce170eed |
| Source note | uspto-grants-1996_09 |