HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylpropylamine → N-(3-Phenylpropyl)-3-(1H-imidazol-4-yl)propanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylpropylamine | HCID 16259 | — |
| Reactant | HCID 178525356 | HCID 178525356 | — |
| Product | N-(3-Phenylpropyl)-3-(1H-imidazol-4-yl)propanamide | HCID 178520519 | — |
Reaction Steps
The preparation is carried out as in Example 1 with 3-phenylpropanamine and 3-(1H-imidazol-4-yl)propanoic acid, the acid being here added after the reaction of the amine component with N,N'-carbonyldiimidazole. The title compound is extracted from water with diethyl ether, purified by chromatography and recrystallized in the hydrogenmaleate form from ethanol/diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05559113 |
| Source dataset | uspto-grants-1996_09 |
| ORD ID | ord-424f81e7bb5f47f0b2ca280258f28261 |
| Source note | uspto-grants-1996_09 |