Methanesulfonyl chloride → HCID 22853533, compound

HRID 744113Notes

Reaction equation

Cl.[CH2:2]([S:6]([NH:9][C@@H:10]([CH2:15][NH2:16])[C:11]([O:13][CH3:14])=[O:12])(=[O:8])=[O:7])CCC.CS([Cl:21])(=O)=O>>[ClH:21].[CH3:2][S:6]([NH:9][C@@H:10]([CH2:15][NH2:16])[C:11]([O:13][CH3:14])=[O:12])(=[O:8])=[O:7]

Participants

Reactant 2

HCID 31297Methanesulfonyl chloride

HCID 22853531HCID 22853531, compound

Product 1

HCID 22853533HCID 22853533, compound

Procedure

5-7 was prepared as described above for the butylsulfonylamino analog (5-6) using methanesulfonyl chloride at the appropriate stage.

Workup

custom5-7 was prepared

Sources & evidence

ORD record: ord-c432c64d16604ca58e0b4be4eaa2862f
Source dataset: uspto-grants-1996_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05559127

Reaction notes

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