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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 744595Generated: October 30, 2026

Methyl iodide → 131988-13-1

https://huagongshe.com/reaction/744595

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 15180132HCID 15180132—
SolventAcetoneHCID 180—
Product131988-13-1HCID 15819045—

Reaction Steps

A mixture of methyl iodide (0.37 ml, 6 mmol) and 3-(4-propoxy-1,2,5-thiadiazol-3-yl)pyridine (700 mg, 3.1 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.98 g (88%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05559138
Source datasetuspto-grants-1996_09
ORD IDord-7730c24cbb17449fa9cd9191cfd12a8a
Source noteuspto-grants-1996_09