Methyl iodide → HCID 19075414, compound

HRID 744604Notes

Reaction equation

HRID 744604 reaction equation
[CH3:1][I:2].[CH2:3]([O:7][C:8]1[C:9]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH:4]([CH3:6])[CH3:5]>CC(C)=O>[I-:2].[CH2:3]([O:7][C:8]1[C:9]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH:4]([CH3:6])[CH3:5]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075496HCID 19075496, compound

Product 1

HCID 19075414HCID 19075414, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.6 ml, 10 mmol) and 3-(4-isobutoxy-1,2,5-thiadiazol-3-yl)pyridine (588 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.88 g (87%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.88 g (87%)

Sources & evidence

ORD record
ord-49276e5de8f74ca681e9f9874d04e9a9
Source dataset
uspto-grants-1996_09
Patent number
US05559138

Reaction notes

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