Methyl iodide → 131988-31-3

HRID 744628Notes

Reaction equation

HRID 744628 reaction equation
[CH3:1][I:2].[CH2:3]([O:11][C:12]1[C:13]([C:17]2[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=2)=[N:14][S:15][N:16]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]>CC(C)=O>[I-:2].[CH2:3]([O:11][C:12]1[C:13]([C:17]2[CH:18]=[N+:19]([CH3:1])[CH:20]=[CH:21][CH:22]=2)=[N:14][S:15][N:16]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180137HCID 15180137, compound

Product 1

HCID 19075404131988-31-3

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (1 ml, 15 mmol) and 3-(4-octyloxy-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.81 g (62%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.81 g (62%)

Sources & evidence

ORD record
ord-5224650be37e4a07aba28e86d236789f
Source dataset
uspto-grants-1996_09
Patent number
US05559138

Reaction notes

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