Methyl iodide → HCID 19075417, compound

HRID 744644Notes

Reaction equation

HRID 744644 reaction equation
[CH3:1][I:2].[S:3]1[N:7]=[CH:6][C:5]([C:8]2[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=2)=[N:4]1>CC(C)=O>[I-:2].[S:3]1[N:7]=[CH:6][C:5]([C:8]2[CH:9]=[N+:10]([CH3:1])[CH:11]=[CH:12][CH:13]=2)=[N:4]1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180168HCID 15180168, compound

Product 1

HCID 19075417HCID 19075417, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (1 ml, 15 mmol) and 3-(1,2,5-thiadiazol-3-yl)pyridine (6 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 1.2 g (74%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 1.2 g (74%)

Sources & evidence

ORD record
ord-22b03f879bbf4bbbb677e27b4aae4691
Source dataset
uspto-grants-1996_09
Patent number
US05559138

Reaction notes

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